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학술저널

입체선택적인 분자내 [2+2] 환화반응을 이용한 광학활성 Bicyclo[4.2.0]octanone의 합성

Synthesis of The Optically Active Bicyclo[4.2.0]octanone by Stereoselective Intramolecular[2+2]Cycloaddition

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Stereoselective synthesis of the optically active bicyclo [4.2.0] octanone 5 was accomplished using intramolecular olefin-keteniminium salt[2+2]cycloaddition of the amide 4 as a key step. This important chiral synthon was prepared starting from readily available L-glutamic acid via an efficient 8-step sequence.

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