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Hexyltriphenylphosphonium-TCNQ 錯物의 合成과 분산용매 중에서의 안정성

Synthesis of Hexyltriphenylphosphonium-TCNQ Complex and Stability in Spreading Solvent

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Hexyltriphenylphosphonium-TCNQ(HTPP-TCNQ) complex for preparing organic thin film by Langmuir-Blodgett technique was synthesized from LiTCNQ and Hexyltriphenylphosphonium bromide. The structure of the new complex was confirmed by ¹H NMR, ³¹P NMR, IR, UV spectroscopies, TGA and elemental analysis. A stability to spreading solvent, which is acetonitrile, ethylacetate, ethanol and acetonitrile-ethylacetate(1:1 v/v), of HTPP-TCNQ complex was investigated by UV-visible spectrophotometer. The complex was stabilized in acetonitrile, ethylacetate, aceton, acetonitrile-ethylacetate(1:1 v/v) for 6 h.

ABSTRACT

I. 서론

II. 실험

III. 결과 및 고찰

IV. 결론

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