ICP-OES를 이용한 우유의 Selenium 분석
- 한국축산식품학회
- Food Science of Animal Resources
- Korean Journal for Food Science of Animal Resources 제23권 제4호
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2003.12356 - 360 (5 pages)
- 이용수 19
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초록
The purpose of this paper was to determine the quantity of selenium in milk by inductively coupled plasma optical emission spectrometry. The sample was digested in teflon vessel containing nitric-hydrogen peroxide acid mixture. After digestion, the sample in treated with additional hydrochloric acid. Total selenium was reduced with sodium borohydride and concentrated hydrochloric acid in a simplified hydride generation(HG) manifold. The optimum conditions of HG are 2 M for HCI, 1.5% for NaBH₄ 1.2mL/min for sample flow. Recovery rates by the standard addition method were 88.0% at 10 ppb and 92.2% at 10 ppm. The relative standard deviations were 4.8 and 3.2%, respectively. This method showed a good accuracy and precision. And so it was highly suitable for determination of small quantity of selenium in milk.
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